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Producing Chlorination-Grade Feedstock from Domestic Ilmenite - Laboratory and Pilot Plant Studies.


PB86171113

Publication Date 1986
Personal Author Elger, G. W.; Wright, J. B.; Tress, J. E.; Bell, H. E.; Jordan, R. R.
Page Count 32
Abstract The Bureau of Mines investigated the conversion, at both laboratory and pilot plant scale, of a low-grade ilmenite to chlorination-grade feedstock that could substitute for imported rutile used to produce titanium tetrachloride. The concentrate was derived from the Tahawus, NY, lode deposit of ilmenite-magnetite in rock that contains anorthosite and gabbro. Charges of the ilmenite concentrate, containing 46.6 wt pct TiO2 blended with soda ash, were carbothermically reduced in an electric arc furnace, which separated most of the iron and left a high-titanium slag. However, the slag contained Ca, Mg, and Mn constituents that rendered the material unsuitable for continuous chlorination by causing plugging problems. After being ground and pelletized, the slag was reacted with SO2 and air at 700 to 900 C, which selectively converted the harmful impurities to soluble compounds that were removed in a subsequent water or dilute HCl leach.
Keywords
  • Ilmenite
  • Extractive metallurgy
  • Titanium oxides
  • Slags
  • Upgrading
Source Agency
  • Bureau of Mines
NTIS Subject Category
  • 71N - Nonferrous Metals & Alloys
  • 48A - Mineral Industries
Corporate Authors Bureau of Mines, Albany, OR. Albany Research Center.
Supplemental Notes Library of Congress catalog card no. 85-600234.
Document Type Technical Report
Title Note Rept of investigations/1986.
NTIS Issue Number 198612
Producing Chlorination-Grade Feedstock from Domestic Ilmenite - Laboratory and Pilot Plant Studies.
Producing Chlorination-Grade Feedstock from Domestic Ilmenite - Laboratory and Pilot Plant Studies.
PB86171113

  • Ilmenite
  • Extractive metallurgy
  • Titanium oxides
  • Slags
  • Upgrading
  • Bureau of Mines
  • 71N - Nonferrous Metals & Alloys
  • 48A - Mineral Industries
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