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Determination of 2,3,7,8-TCDD (Tetrachlorodibenzo-p-Dioxin) in Industrial and Municipal Wastewaters, Method 613. Part 1. Development and Detection Limits.


PB83171280

Publication Date 1983
Personal Author Longbottom, J. E.; Foerst, D. L.; Wesselman, R. J.; Wong, A. S.; McMillin, C. R.
Page Count 26
Abstract A convenient method for water and wastewater samples is presented that will determine 2,3,7,8-TCDD concentrations to a Method Detection Limit (MDL) of 2 ng/L. The method uses solvent extraction of the aqueous sample followed by capillary column gas chromatography/mass spectrometry using Selected Ion Monitoring. The capillary column (Silar 10C or equivalent) is isomer specific for 2,3,7,8-TCDD.
Keywords
  • Water analysis
  • Industrial wastes
  • Sewage
  • Pesticides
  • Herbicides
  • Chemical analysis
  • Chlorine organic compounds
  • Solvent extraction
  • Gas chromatography
  • Mass spectroscopy
  • Reprints
  • Dibenzodioxin/tetrachloro
  • Water pollution detection
Source Agency
  • Environmental Protection Agency Office of Research and Development
NTIS Subject Category
  • 68E - Pesticides Pollution & Control
  • 99A - Analytical Chemistry
  • 68D - Water Pollution & Control
Corporate Authors Environmental Monitoring and Support Lab.-Cincinnati, OH.
Supplemental Notes Prepared in cooperation with California Analytical Lab., Inc., Sacramento, CA., and Monsanto Research Corp., Dayton, OH. Dayton Lab.
Document Type Journal Article
NTIS Issue Number 198313
Determination of 2,3,7,8-TCDD (Tetrachlorodibenzo-p-Dioxin) in Industrial and Municipal Wastewaters, Method 613. Part 1. Development and Detection Limits.
Determination of 2,3,7,8-TCDD (Tetrachlorodibenzo-p-Dioxin) in Industrial and Municipal Wastewaters, Method 613. Part 1. Development and Detection Limits.
PB83171280

  • Water analysis
  • Industrial wastes
  • Sewage
  • Pesticides
  • Herbicides
  • Chemical analysis
  • Chlorine organic compounds
  • Solvent extraction
  • Gas chromatography
  • Mass spectroscopy
  • Reprints
  • Dibenzodioxin/tetrachloro
  • Water pollution detection
  • Environmental Protection Agency Office of Research and Development
  • 68E - Pesticides Pollution & Control
  • 99A - Analytical Chemistry
  • 68D - Water Pollution & Control
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