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Synthesis of Trifluoromethylsulfur Pentafluoride (CF3SF5).


PB233149

Publication Date 1974
Personal Author Tyczkowski, E. A.
Page Count 16
Abstract A quantity of 100 lb. of CF3SF5 was prepared by the cobalt trifluoride fluorination of bis(trifluoromethyl)disulfide (CF3SSCF3). It was purified by alkaline sulfite scrubbing and fractional distillation to meet the quality requirements.
Keywords
  • Fluorination
  • Organic sulfides
  • Synthesis(Chemistry)
  • Purification
  • Fluorine organic compounds
  • Sulfur fluorides
  • Cobalt fluorides
  • Sulfur/pentafluoro-trifluoromethyl
Source Agency
  • Office of Research and Monitoring
NTIS Subject Category
  • 99D - Basic & Synthetic Chemistry
Corporate Authors Armageddon Chemical Co., Durham, N.C.
Document Type Technical Report
Title Note Environmental Monitoring series (Final) 24 Aug 72-12 Jan 74.
NTIS Issue Number 197417
Contract Number
  • EPA-68-02-0680
Synthesis of Trifluoromethylsulfur Pentafluoride (CF3SF5).
Synthesis of Trifluoromethylsulfur Pentafluoride (CF3SF5).
PB233149

  • Fluorination
  • Organic sulfides
  • Synthesis(Chemistry)
  • Purification
  • Fluorine organic compounds
  • Sulfur fluorides
  • Cobalt fluorides
  • Sulfur/pentafluoro-trifluoromethyl
  • Office of Research and Monitoring
  • 99D - Basic & Synthetic Chemistry
  • EPA-68-02-0680
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